Production and characterization of a new biodegradable fenugreek seed gum based active nanocomposite film reinforced with nanoclays


Memiş S., TÖRNÜK F., BOZKURT F., Durak M. Z.

International Journal of Biological Macromolecules, cilt.103, ss.669-675, 2017 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 103
  • Basım Tarihi: 2017
  • Doi Numarası: 10.1016/j.ijbiomac.2017.05.090
  • Dergi Adı: International Journal of Biological Macromolecules
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.669-675
  • Anahtar Kelimeler: Film properties, Nanofiller, Polymer reinforcement
  • Sivas Cumhuriyet Üniversitesi Adresli: Hayır

Özet

In the present work, fenugreek seed gum (FSG)/clay nanocomposite films were prepared with nanoclays (Na+ montmorillonite [MMT], halloysite [HNT] and Nanomer® I.44 P [NM]) at different amounts (0, 2.5, 5.0 and 7.5 g clay/100 g FSG) by solution casting method and characterized. Increasing amount of nanoclay significantly (P < 0.05) improved oxygen barrier and thermal properties of the biodegradable films. Agar diffusion tests revealed that FSG based nanocomposite films exhibited strong antimicrobial properties against foodborne pathogens namely Listeria monocytogenes, Escherichia coli O157:H7, Staphylococcus aureus and Bacillus cereus independently of clay type and concentration. In the case of mechanical properties, nanoclay incorporation up to 5% provided higher (P < 0.05) tensile strength (TS) properties while elongation at break (EB) values of the films significantly (P < 0.05) decreased in the presence of clay in the film matrix. SEM micrographs showed that especially lower levels (up to 5%) of nanoclay reinforcements provided a homogeneous and smooth film structure. In conclusion, FSG based nanocomposite films reinforced with nanoclays up to 5% showed a precious potential to be used in antimicrobial food packaging applications.